INGREDIENTS

INSTRUCTIONS

To a 2-L jacketed round reactor vessel (reactor #1) with an overall heat
transfer coefficient of about 100 Btu/F-ft2-hr, add ingredients one, two
and three with constant agitation.
In a second 2-L reactor vessel with a radial flow impeller operating at 100
rpm, add ingredients four, five, six, and seven until the mixture is
homogenous.
To reactor #2, add ingredient eight, followed by three equal volumes of the
homogenous mixture in reactor #1. Additionally, add ingredient nine and ten
slowly, with constant agitation. Care must be taken at this point in the
reaction to control any temperature rise that may be the result of an
exothermic reaction.
Using a screw extrude attached to a #4 nodulizer, place the mixture
piece-meal on a 316SS sheet (300 X 600 mm). Heat in a 460K oven for a
period of time that is in agreement with Frank & Johnston's first order
rate expression (see JACOS, 21,55), or until golden brown. Once the
reaction is complete, place the sheet on a 25C heat-transfer table,
allowing the product to come to equilibrium.
Recipe by: WHY ENGINEERS DON'T WRITE RECIPES Posted to MC-Recipe Digest V1
#686 by Creedenite@aol.com on Jul 21, 1997

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